{"id":728,"date":"2024-03-02T22:17:06","date_gmt":"2024-03-02T14:17:06","guid":{"rendered":"https:\/\/factory.sslab.org.cn\/sxxjdc\/?p=728"},"modified":"2024-07-29T15:42:05","modified_gmt":"2024-07-29T07:42:05","slug":"%e5%bc%80%e5%8f%91%e9%ab%98%e8%83%bd%e9%87%8f%e5%af%86%e5%ba%a6%e9%94%8c%e7%a2%98%e7%94%b5%e6%b1%a0%e6%9e%84%e5%bb%ba%e7%bc%ba%e7%94%b5%e8%8d%b7%e6%80%81%e9%98%b4%e6%9e%81%e6%9d%90%e6%96%99%e4%bb%a5","status":"publish","type":"post","link":"https:\/\/factory.sslab.org.cn\/sxxjdc\/blog\/2024\/03\/02\/%e5%bc%80%e5%8f%91%e9%ab%98%e8%83%bd%e9%87%8f%e5%af%86%e5%ba%a6%e9%94%8c%e7%a2%98%e7%94%b5%e6%b1%a0%e6%9e%84%e5%bb%ba%e7%bc%ba%e7%94%b5%e8%8d%b7%e6%80%81%e9%98%b4%e6%9e%81%e6%9d%90%e6%96%99%e4%bb%a5\/","title":{"rendered":"\u5f00\u53d1\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u950c\u7898\u7535\u6c60:\u6784\u5efa\u7f3a\u7535\u8377\u6001\u9634\u6781\u6750\u6599\u4ee5\u50ac\u5316\u950c\u7898\u53cc\u7535\u5b50\u5e73\u53f0\u884c\u4e3a"},"content":{"rendered":"
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TOC. \u50ac\u5316\u673a\u7406\u793a\u610f\u56fe<\/figcaption><\/figure><\/div>\n\n
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\u56fe 1. \u50ac\u5316\u5242\u7684\u7ed3\u6784\u9610\u91ca\u548c\u57fa\u672c\u7279\u5f81\u3002a) Co9<\/sub>S8<\/sub>@NC \u7684XRD\u56fe\u3002 b) Co9<\/sub>S8<\/sub>@NC \u7684 N2 \u5438\u9644-\u8131\u9644\u7b49\u6e29\u7ebf\uff0c\u63d2\u56fe\u4e3a\u76f8\u5e94\u7684\u5b54\u5f84\u5206\u5e03\u3002d) \u4e0e UPS \u7ed3\u679c\u76f8\u5bf9\u5e94\u7684 Co9<\/sub>S8<\/sub>@NC \u7684\u529f\u51fd\u6570\u56fe\u3002 e-f) \u5355\u5206\u6563 Co9<\/sub>S8<\/sub> \u5728\u591a\u5b54 NC \u6846\u67b6\u4e0a\u7684 SEM \u56fe\u50cf\u548c TEM \u56fe\u50cf\u3002 g) \u5177\u6709\u6838\u58f3\u6784\u578b\u7684 Co9<\/sub>S8<\/sub>@NC \u7684 HRTEM \u56fe\u50cf\u3002<\/figcaption><\/figure><\/div>\n\n
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\u56fe 2. I+<\/sup>\/I0<\/sup>\/I–<\/sup> \u8f6c\u5316\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u6d3b\u5316\u80fd\u7684\u53d8\u5316\u3002 a) \u5206\u522b\u57fa\u4e8eCo9<\/sub>S8<\/sub>@NC \u7535\u6781\u548c NC \u7535\u6781\u7684 I+<\/sup>\/I0<\/sup>\/I–<\/sup> \u53cd\u5e94\u548c I0<\/sup>\/I–<\/sup> \u53cd\u5e94\u7684\u653e\u7535\u66f2\u7ebf\u3002\u7535\u6c60\u7b26\u53f7\u4ee3\u8868\u57fa\u4e8e\u5355\u7535\u5b50\u8f6c\u79fb\u7684 I0<\/sup>\/I–<\/sup> \u53cd\u5e94\u7684\u80fd\u91cf\u5bc6\u5ea6\u3002\u63d2\u56fe\u4e3a\u7b49\u6548\u7535\u8def\uff0c\u5176\u4e2d RS \u4e3a\u56fa\u6709\u6b27\u59c6\u7535\u963b\uff0cRCT \u4e3a\u7535\u8377\u8f6c\u79fb\u7535\u963b\uff0cZW \u4e3a\u79bb\u5b50\u6269\u6563\u7535\u963b\uff0cCPE \u4e3a\u7535\u8377\u8f6c\u79fb\u8fc7\u7a0b\u4ea7\u751f\u7684\u7535\u5bb9\u3002 c) Co9<\/sub>S8<\/sub>@NC \u7535\u6781\u548c NC \u7535\u6781\u5728 1.7 V \u65f6\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684 RCT\u3002d) \u5728 1 V \u81f3 1.7 V \u7684\u7535\u538b\u8303\u56f4\u5185\uff0c\u7535\u8377\u8f6c\u79fb\u7535\u963b\u7684\u5bf9\u6570\u4e0e\u7edd\u5bf9\u6e29\u5ea6\u7684\u5012\u6570\u4e4b\u95f4\u7684\u7ebf\u6027\u5173\u7cfb\u3002 e) \u5728 1 V \u81f3 1.7 V \u7684\u7535\u538b\u8303\u56f4\u5185\uff0c\u6d3b\u5316\u80fd\u7684\u53d8\u5316\u3002<\/figcaption><\/figure><\/div>\n\n
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\u56fe 3. \u4e0d\u540c\u5de5\u4f5c\u7535\u538b\u72b6\u6001\u548c\u6e29\u5ea6\u4e0b Co9<\/sub>S8<\/sub>@NC \u7535\u6781\u7684\u7535\u5316\u5b66\u6027\u80fd\u548c\u52a8\u529b\u5b66\u5206\u6790\u3002 a) Co9<\/sub>S8<\/sub>@NC \u7535\u6781\u548c NC \u7535\u6781\u5728 0.1 mV s-1 \u4e0b\u7684 CV \u66f2\u7ebf\u3002c) LSV \u5f97\u51fa\u7684 I+<\/sup>\/I0<\/sup> \u548c I0<\/sup>\/I–<\/sup> \u7684 Tafel \u659c\u7387\u3002 d, e) \u5ba4\u6e29 30 \u00b0C \u548c\u4f4e\u6e29 -30 \u00b0C \u4e0b\u7684\u539f\u4f4d EIS \u7ed3\u679c\u3002<\/figcaption><\/figure><\/div>\n\n
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\u56fe 4. Co9<\/sub>S8<\/sub>@NC \u7535\u6781\u5de5\u4f5c\u673a\u7406\u7684\u50ac\u5316\u5206\u6790\u3002a) \u5145\u7535\u548c\u653e\u7535\u8fc7\u7a0b\u4e2d\u7898\u4e2d\u95f4\u4ea7\u7269\u7684\u539f\u4f4d\u62c9\u66fc\u8868\u5f81\u3002 b) Co9<\/sub>S8<\/sub>@NC \u548c c) NC \u7535\u6781\u4e0a\u5438\u9644\u7684\u7898\u548c\u4e2d\u95f4\u4ea7\u7269\u7684\u7535\u8377\u5bc6\u5ea6\u5dee\u3002d) \u4e0d\u540c\u7898\u7269\u79cd\u5728 Co9<\/sub>S8<\/sub>@NC \u548c NC \u4e0a\u7684\u5438\u9644\u80fd\u3002 e) \u5409\u5e03\u65af\u81ea\u7531\u80fd\u68af\u5f62\u56fe\u3002 f-g) ICl \u548c I2<\/sub> \u5728 Co9<\/sub>S8<\/sub>@NC \u548c NC \u7535\u6781\u4e0a\u7684 PDOS\u3002\u84dd\u8272\u3001\u7ea2\u8272\u548c\u9ed1\u8272\u865a\u7ebf\u5206\u522b\u5bf9\u5e94 p \u6ce2\u6bb5\u4e2d\u5fc3\u3001d \u6ce2\u6bb5\u4e2d\u5fc3\u548c\u8d39\u7c73\u7ea7\u7684\u4f4d\u7f6e\u3002<\/figcaption><\/figure><\/div>\n\n
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\u56fe 6. Zn\u2016I\/ Co9<\/sub>S8<\/sub>@NC \u5728\u4f4e\u6e29\u4e0b\u7684\u7535\u6c60\u6027\u80fd\u3002a) \u5728 -30\u2103 \u4e0b\u4e0d\u540c\u5de5\u4f5c\u7535\u6d41\u4e0b\u7684\u901f\u7387\u6027\u80fd\u3002 b) \u4e0d\u540c\u7535\u6d41\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002 c, d) \u5206\u522b\u5728 1 A g-1<\/sup> \u7684\u4f4e\u7535\u6d41\u548c 5 A g-1<\/sup> \u7684\u9ad8\u7535\u6d41\u4e0b\u7684\u5faa\u73af\u6027\u80fd\u3002e) 3 \u5398\u7c73*4 \u5398\u7c73\u5927\u5c0f\u7684\u8f6f\u7535\u6c60\u7ec4\u56fe\u7247\u3002 f) \u8f6f\u7535\u6c60\u7ec4\u5728\u4f4e\u6e29\u548c\u9ad8\u6e29\u4e0b\u7684\u5faa\u73af\u6027\u80fd\u3002<\/figcaption><\/figure><\/div>\n\n\n

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